The Small-angle scattering like Small-angle X-ray scattering (SAXS) can be used to measure the long periods of semicrystalline polymers.
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Transmission Electron Microscopy in combination with staining techniques, but also Scanning Electron Microscopy, Scanning probe microscopy are important tools to optimize the morphology of materials like polybutadiene-polystyrene polymers and many polymer blends.
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